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Different refiners have a variety of procedures in place for hydroprocessing reactor and reactor system shutdowns, depending on the scope of the work to be performed during the downtime. If activities are to be performed inside the reactor (e.g. inspection, maintenance, catalyst changeout, etc.) such that the reactor must be opened to air, shutdowns must include steps to address the various hazards. These same steps must also be applied to associated process equipment related to the reactor system susceptible to similar hazards and damage mechanisms.
The stress corrosion cracking (SCC) behavior of Fe13Cr5Ni- and Fe17Cr5.5Ni-based alloys in HTHP CO2 environments was investigated through slow strain rate tests (SSRT) and electrochemical methods. The results show that a remarkable decrease in tensile strength and elongation to failure was observed when testing in CO2 environment as compared with air. Fe17Cr5.5Ni-based alloys possessed better SCC resistance than Fe13Cr5Ni-based alloys. The increase of Cr and Ni content tended to enhance the resistance to SCC and pitting corrosion. The SCC behaviors of Fe13Cr5Ni- and Fe17Cr5.5Ni-based alloys were closely associated with the repassivation capacity and the resistance to pitting corrosion.
On March 2011 at Fukushima Daiichi NPS, seawater was injected into spent fuel pools just after the accident for emergency cooling. The temperature of the water in a pool raised up to 93 ℃, and the chloride ion concentration raised up to 1,944 ppm (maximum) after seawater injection. In this high temperature and high chloride ion concentration environment, localized corrosion including crevice corrosion may have occurred on components made of passive metals such as stainless steels. The environment is assumed to be susceptible to crevice corrosion for 304 SS based on laboratory experiments and the concept of ER, CREV. There is a low possibility of initiating localized corrosion after the water was purified and deoxygenated. However, it is not certain whether localized corrosion, once initiated and propagated under the severe condition, will repassivate after the bulk water is purified. It is necessary to examine the continuity of crevice corrosion propagation when the bulk water is purified and deaerated, which means the cathodic reactions outside the crevice will no longer contribute to the propagation of the corrosion.
Food consists mainly of proteins, carbohydrates, and fats. Processed foods contain diverse aqueous solutions, syrups, and additives, used to improve food appearance, taste, quality and preservation. They have a wide pH range, components such as, salt, water, and vinegar impact food corrosivity.
M. B. Kermani pointed out that 25% of equipment failures in the oil and gas industry are caused by corrosion, and more than half of corrosion events are related to produced fluids containing CO2 and H2S. In recent years, the exploitation of sour oil and gas fields (containing H2S or H2S/CO2 mixture) has become more and more common, and prominent problems such as tubing ruptures caused by pitting and uniform corrosion have appeared. In oil fields containing CO2 and H2S, local corrosion is a key factor restricting the selection of tubing and casing materials. In an oilfield containing CO2 and H2S in the Middle East, the authors corroded coupons on site, and carried out indoor simulation experiments for the problems found in the field test. The authors systematically studied 13Cr, S13Cr, 22Cr, 25Cr and 2550 in the presence of H2S, CO2 and high mineralization.
Electrochemical techniques enabling real-time survey of corrosion, such as multi-electrode arrays sensors (MASS) and linear polarization resistance (LPR) were used to detect the differences in electrochemical behavior of two stainless steels.
Experiments to determine the critical pitting temperature of several alloys in calcium bromide solutions using the ASTM G150 electrochemical critical pitting test procedures. Similar experiments were also conducted in solutions containing equal concentrations (by weight) of chlorides and bromide.
With the rapid economic development and the dramatic population growth, the demand on clean energy is continuously increasing.1 Due to the depletion of conventional crude oil reserves, the unconventional oil resources such as oil sands become more attractive.2 Canada has a total estimated oil sands reserves of 161.4 billion barrels by the end of 2020, accounting for 9.3% of the global reserves.3 The bitumen in the oil sands is extracted and transported through pipelines to the refineries with refining capabilities in Canada and the United States where the raw bitumen is processed to produce marketable synthetic crude oil (SCO). The proposed TransCanada system planned to connect the Alberta bituminous oil sands to the refineries as far as in Texas.4
Hydrothermal liquefaction (HTL) of wet and waste biomass feedstocks into crude bio-oils and other chemicals has attracted particular attention in Canadian and international clean energy sectors. Until today, very little effort has been employed to address corrosion problems of HTL core components under operation, leading to a significant delay in the construction of industrial-scale HTL plants. In fact, a range of oxygenated, aggressive sulfur and/or chlorinated compounds, as well as organic acids, can be introduced during the conversion at the operating temperature range of 200–400℃, consequently creating highly corrosive environments to the reactor alloys. It is thus important to investigate the performance of alloys exposed to conversion processes to determine the cost-effective construction and long-term safe operation of the HTL plants. In this study, the corrosion resistance of two candidate austenitic stainless steels, including UNS S31000 and UNS S31603, was assessed in a batch reactor containing bamboo feedstock. The corrosion behaviors of the austenitic stainless steels were evaluated using weight change measurement methods and advanced microscopy techniques. To advance corrosion mechanistic understanding, the chemistry of conversion products was also analyzed. This paper is a summary of our most recent results obtained.