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The four-point bend test as per NACE TM0316-2016 is used in the oil and gas industry as a common test to evaluate the resistance of line pipe steels to sulfide stress cracking. The appearance of stressinduced pits or grooves on the test specimens can sometimes be noted when testing is performed under high load, at low pH or in CO2 containing test environments. When evaluating SSC specimens, it is important to distinguish between stress-induced corrosion pits and SSC crack structures and their relevance for the SSC test result. Within this study a systematic investigation of the level of applied stress, the test gas composition and the surface finish of test specimens and their influence on the onset and growth of cracking of four-point bend SSC specimens was performed. In this context the role of shape and maximum depth of stressinduced corrosion pits and stress grooves are discussed in detail.
Key words: SSC, Four-Point Bend Test
Steel pipelines are sometimes subjected to demanding sour environments resulting from the presence of high H2S contents. Pipeline materials, therefore, must be resilient against sulfide stress cracking (SSC) which is caused by H2S. Beginning in the 1980s, thermo-mechanically controlled processed (TMCP) steels have been widely used for the manufacturing of large-diameter sour service pipelines. The failure of the Kashagan pipelines in 2013 raised concern regarding the use of TMCP steels in sour environments. These concerns arise from the potential for local hard zones (LHZs) to be produced on the surface of the line pipe during TMCP processes, ultimately leading to through-wall SSC failures. In the present study, several X60 - X65 TMCP steels (both with and without LHZs) have been tested under different Region 3 (R3) conditions in the NACE MR0175/ISO15156-2 pH-H2S partial pressure diagram. It can be concluded that the presence of LHZs increases TMCP steels’ sour cracking susceptibility; however, TMCP steels without LHZs pass the SSC tests at even the most severe R3 environments. Traditional HRC or HV10 testing are not able to detect LHZs, and so lower load HV 0.5 or HV 0.1 tests are necessary. For TMCP steels, the current R3 may be further divided into R3-a and R3-b sub-regions. The sour cracking severity of R3-a is less than that of R3-b. Additional actions, like enhanced mill qualification of the TMCP plate, should be considered to ensure that no LHZs exist in steels to be utilized in R3-b environments.
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