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Recent results of sour gas and hydrogen embrittlement testing of CW N07022 alloy will be presented. The test results of CW N07022 alloy will demonstrate that it offers superior properties to precipitation-strengthened Ni-base alloys for demanding oil and gas applications.
N07022 is a Ni-21Cr-17Mo (wt.%) alloy that has found success in applications requiring corrosion resistance and high strength which it achieves in the cold-worked condition. The attributes of N07022 alloy make it an excellent candidate for many oil and gas applications. It has been incorporated in the NACE MR0175 / ISO15156 and NACE MR0103 / ISO 17945 standards at the highest test levels. It has also shown resistance to the NACE Level VII environment with 5 g/L elemental sulfur at 205°C (401°F) and to the demanding conditions of 25% NaCl + 1000 psi (6.9 MPa) CO2 + 1000 psi (6.9 MPa) H2S at 288°C (550°F). As higher strength alloys are becoming more common in high-pressure high-temperature (HPHT) oil and gas service there have been a number of reported failures involving precipitation-strengthened Ni-base alloys. These failures were attributed to hydrogen embrittlement. Recent results of sour gas and hydrogen embrittlement testing of cold-worked N07022 alloy will be presented. The test results and properties of cold-worked N07022 alloy will be compared to those for precipitation-strengthened Ni-base alloys. Overall the results demonstrate that N07022 alloy is currently the best alloy for demanding oil and gas applications.
Key words: Nickel-Base Alloys, Ni-Cr-Mo, N07022, C-22HS, Cold Work, NACE MR0175, Sour Gas, Hydrogen Embrittlement
Materials qualification testing of corrosion resistant alloys (CRAs) typically involves the use of simple pass/fail tests. Modification of existing standards is recommended for environments in which pit initiation is statistically improbable but pit propagation is rapid, e.g. low chloride/high H2S.
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Stress Oriented Hydrogen Induced Cracking (SOHIC) susceptibility of SA516 Grade 70 carbon-manganese steel was studied according to NACE MR0175/ISO15156-2 standard by four-point-bending and constant load test methods. Base metal and welded specimens were investigated.
A test project to examine the susceptibility of Hydrogen Induced Stress Cracking (HISC) has been executed. In this project hydrogen charged samples of Alloy 718 and Alloy 725 have been exposed under tensile stress to establish critical stress levels for initiation of HISC.