Search
Filters
Close

Products tagged with 'pitting corrosion'

View as
Sort by
Display per page
Picture for Effect of Heat Treatment and Manufacturing Method on the Susceptibility to Hydrogen Induced Stress Cracking of UNS N06625
Available for download

Effect of Heat Treatment and Manufacturing Method on the Susceptibility to Hydrogen Induced Stress Cracking of UNS N06625

Product Number: 51324-20899-SG
Author: Eivind Bruun Thorstensen; Atle Helge Qvale; Vebjørn Andresen ; Roy Johnsen; Paal Bratland
Publication Date: 2024
$40.00
This paper presents results obtained from examining the effect of heat treatment and production method on the hydrogen induced stress cracking (HISC) susceptibility of UNS N06625 (Alloy 625). Five different versions of Alloy 625 were examined: Hot forged material heat treated at 920 °C, 1010 °C and 1100 °C respectively, material produced by hot isostatic pressing (HIP) and material that has been solution annealed and strain hardened (cold worked) at a temperature below secondary phase formation. The different versions of Alloy 625 were initially characterized by identifying the critical pitting temperature (CPT) by use of a modified ASTM G48 Method C test. Resistance to Hydrogen Embrittlement (HE) has been examined by use of stepwise loading of tensile specimens in a hydrogen charging environment in CortestTM proof rings, followed by fractography characterization and microstructural examination by use of Optical Light Microscope (OLM) and Scanning Electron Microscope (SEM). The hot forged and the HIP’ed versions of Alloy 625 that subsequently were heat treated, were found to be susceptible to HISC. The evaluation was based on a decrease in strength and ductility, as well as brittle fracture surfaces and secondary cracking on the samples’ outer surface. Among the hot forged and heat-treated versions, the samples heat treated at 1010°C were found to be the most susceptible to HISC, while (solution) heat treatment at 1100°C resulted in the lowest HISC susceptibility amongst the hot forged and heat-treated qualities. The solution annealed (1150 °C) and cold worked version showed a higher resistance to HISC, as no reduction in fracture strength, nor any secondary cracking were observed. The amount of grain boundary precipitations was found to be the main factor influencing the HISC susceptibility, where an increased amount of grain boundary precipitations led to higher susceptibility. The effect of grain size on the HISC susceptibility of samples charged with hydrogen were also considered, and the results indicate that larger grains have a beneficial effect on the ductility.
	Picture for Erosion and Corrosion Assessment of Type 304L Stainless Steel Jumper Removed from Nuclear Waste Transfer Service
Available for download

Erosion and Corrosion Assessment of Type 304L Stainless Steel Jumper Removed from Nuclear Waste Transfer Service

Product Number: 51324-20634-SG
Author: Sheewa X. Feng; Jason S. Page
Publication Date: 2024
$40.00
A pipe connection assembly (jumper), fabricated from Type 304L stainless steel, was used to transfer nuclear waste from one tank to other tanks on the Hanford Site. After serving as the routing connection for approximately 11 million liters of tank waste over approximately 11 months, the jumper was removed from service and examined to determine any erosion, pitting, cracking, or other forms of degradation to the jumper. Ultrasonic transducer measurements for wall thickness before and after service at the same selected locations show that there was no measurable wall loss, and no erosion patterns were observed. After the ultrasonic transducer measurement, the jumper section was cut open to expose the inner surface for detailed examination by optical microscopy and scanning electron microscopy. The straight pipe sections at both upstream and downstream locations looked pristine, while discoloring was observed at the two welds, in the heat-affected zone, and in nearby regions joining the elbow and straight pipes. There was no erosion, pitting corrosion, or flow-induced corrosion, nor were there other corrosion mechanisms in evidence except for a crack-like feature observed at the boundary of the base metal and weld. Material etching didn't show alignment of the crack with grain boundaries. Degree of sensitization measurement shows that the weld and heat-affected zone, including the neighboring base, was only slightly sensitized during the manufacturing process. The results suggest that there is very low likelihood that the crack-like feature observed from the weld cross section was the result of stress corrosion cracking. Overall, the jumper performed well during the waste transfer process.