Server maintenance is scheduled for Saturday, December 21st between 6am-10am CST.
During that time, parts of our website will be affected until maintenance is completed. Thank you for your patience.
Use GIVING24 at checkout to save 20% on eCourses and books (some exclusions apply)!
The specimen surface, effect of filling rate were examined. Characterization of the primary fracture surface and the gauge section of the tested specimens was done by scanning electron microscopy and subsequent classification according to the NACE TM0198 standard.
The slow strain rate test (SSRT) is a method of screening corrosion resistant alloys (CRAs) for resistance to stress corrosion cracking at elevated temperatures in sour oilfield production environments. Moreover it is used as a quality control test included as a part of the material specification requirements because of the short time to obtain results.However there are some issues related to the performance of the testing and the characterization of the tested specimens which have a direct impact on the final result of the test. The purpose of this paper is to highlight some of these difficulties encountered during the testing of different CRAs grades such as N08028 N08535 and N08825. One of these issues is the influence of the final grinding of the specimen (grit paper number longitudinal or transversal grinding lubrication…) to have a proper surface finish which does not affect the performance of the material during the testing. A second problem is the method of pressurizing the autoclave to reach a repetitive value of the gas total pressure at elevated temperatures. In this sense some testing procedures establish the value of H2S pressure at room temperature but do not specify what should be the condition in the autoclave in testing condition. Taking account of that it appears to be a big challenge to test the material exactly at the same conditions when autoclaves of different sizes and shapes are implied in the testing. Once the test is finished other problems arise related to the tested specimen characterization. One of them is the accuracy in the measurement of the reduction of area which is a critical parameter to classify the result of the test. In addition regarding the visual examination of the test specimen NACE TM0198 proposes four different classes depending on the features observed on the primary fracture surface and the type of secondary cracks in the gauge section that may be not easily attributes. Another problem appears when the ductility ratios are above 0.8 where a further analysis on cross sections is required by scanning electron microscopy (SEM) in order to distinguish fissures from SCC secondary cracking focussed in the necked region. To complete the tested specimen characterization a deep evaluation of the primary fracture by SEM has been performed with slight loss of ductility (<20%) for the three grades. Special features have been observed; some of them clearly related with SCC and some others of more difficult interpretation.Slow strain rate testing is a rapid method with a strong potential for ranking alloys for material selection purposes. However it is a test method subjected to different issues that may affect the results and lead to inconsistent conclusions.
Key words: slow strain rate test, corrosion-resistant alloys, specimen preparation, reduction in area measurement, fracture surface characterization, filling rate, testing pressure
Over 5 years, 70 to 80 FGD scrubber units have exhibited corrosion problems. Many were after only a few months of service. This paper will provide an overview of readily available technical information in the published literature and past experience that could have been used to minimize corrosion problems in these FGD units.
We are unable to complete this action. Please try again at a later time.
If this error continues to occur, please contact AMPP Customer Support for assistance.
Error Message:
Please login to use Standards Credits*
* AMPP Members receive Standards Credits in order to redeem eligible Standards and Reports in the Store
You are not a Member.
AMPP Members enjoy many benefits, including Standards Credits which can be used to redeem eligible Standards and Reports in the Store.
You can visit the Membership Page to learn about the benefits of membership.
You have previously purchased this item.
Go to Downloadable Products in your AMPP Store profile to find this item.
You do not have sufficient Standards Credits to claim this item.
Click on 'ADD TO CART' to purchase this item.
Your Standards Credit(s)
1
Remaining Credits
0
Please review your transaction.
Click on 'REDEEM' to use your Standards Credits to claim this item.
You have successfully redeemed:
Go to Downloadable Products in your AMPP Store Profile to find and download this item.
A series of pitting corrosion and electrochemical tests were performed, aimed at assessing the suitability of UNS S31603 (316L) in an anoxic brine where the chloride concentration was up to 250 000 mg l-1.
Samples simulating the continuous changing structures of UNS S30400 heat affected zone (HAZ) were prepared for examination using metallographic structural analysis, corrosion morphological observations, and traditional electrochemical measurements to characterize the intergranular corrosion and pitting resistance.