The use of carbon steel pipework for aggressive environments in the process industries may often result in premature service lives. This prompts the need to rehabilitate or repair live components before their scheduled shut-downs. The necessity to extend the life of these components has led to the development and use of temporary non-metallic repair systems which must be resistant to the chemical environment. These systems offer cost effectiveness ease of application and may be engineered for specific cases. Measuring the degradation rate of these non-metallic repair systems allows them to be specified for certain applications with confidence. Case studies highlighting successes failures along with laboratory research are presented. This paper will discuss the use of a non-metallic repair system coupled with laboratory research to characterize the degradation of the repair system in various environments. Changes in physical properties after 1000 hr exposure are evaluated through mechanical testing such as modulus change hardness and weight. Changes in chemical composition of the polymer are evaluated through Fourier Transform Infrared spectroscopy (FT-IR). The aqueous mediums chosen included HCL NaOH H2SO4 Acetic Acid and MEK. The results are used to determine the suitability of the materials for the intended service and the load carrying capability.