Celebrate World Corrosion Awareness Day with 20% off eCourses and eBooks with code WCAD2024 at checkout!
Four-point bend testing is used extensively in the oil and gas industry to evaluate resistance of metals to sulfide stress cracking and stress corrosion cracking. The face of the specimen to be tested is stressed in tension and the reverse face in compression. The test is carried out for a specified exposure period with the specimen held under constant displacement using compact loading jigs. The compact nature of the jigs enables testing of several specimens in the test vessel simultaneously. Despite the apparent simplicity of the test, there are many factors that can influence the test results. The purpose of this standard is to establish a reliable methodology for conducting the tests to enhance repeatability and reproducibility of test data. The results of the tests can then be used with greater confidence to rank the performance of metals, the relative aggressiveness of environments, and to provide a basis for qualifying metals for service application. As such, the standard will be of particular benefit to materials and corrosion engineers in the oil and gas sector and to test laboratories providing critical data.
We are unable to complete this action. Please try again at a later time.
If this error continues to occur, please contact AMPP Customer Support for assistance.
Use this error code for reference:
Please login to use Standards Credits*
* AMPP Members receive Standards Credits in order to redeem eligible Standards and Reports in the Store
You are not a Member.
AMPP Members enjoy many benefits, including Standards Credits which can be used to redeem eligible Standards and Reports in the Store.
You can visit the Membership Page to learn about the benefits of membership.
You have previously purchased this item.
Go to Downloadable Products in your AMPP Store profile to find this item.
You do not have sufficient Standards Credits to claim this item.
Click on 'ADD TO CART' to purchase this item.
Your Standards Credit(s)
1
Remaining Credits
0
Please review your transaction.
Click on 'REDEEM' to use your Standards Credits to claim this item.
You have successfully redeemed:
Go to Downloadable Products in your AMPP Store Profile to find and download this item.
Stress corrosion crack (SCC) initiation testing has been performed on a 15% cold-worked UNS N06600 (Alloy 600) heat in mill-annealed (MA), solution annealed (SA), and thermally treated (TT) conditions to assess the role of grain boundary (GB) carbides on stress-assisted intergranular attack (IGA) and short crack nucleation and growth. The SCC initiation tests were conducted at a constant load equivalent to the materials’ yield stress in 360oC simulated pressurized water reactor primary water. Results revealed the highest SCC initiation susceptibility occurred in the Alloy 600 MA material, followed by the TT and SA materials, suggesting that GB carbide distribution did not have a controlling effect on SCC initiation resistance. Quantitative assessments of IGA and short cracks were conducted to help understand this phenomenon, and the role of GB carbides in precursor damage development that leads to differences in macroscopic SCC initiation behavior are discussed.
Methods to protect austenitic stainless steel from polythionic acid stress corrosion cracking (SCC) found to occur during downtimes and contiguous shutdown and start-up periods. Historical Document 1986
Methods to protect austenitic stainless steel and other austenitic alloys from polythionic acid stress corrosion cracking (SCC) occurring during downtimes and contiguous shutdown and start-up periods. Historical Document 1993
Methods to protect austenitic stainless steel and other austenitic alloys from polythionic acid stress corrosion cracking (SCC) occurring during downtimes and contiguous shutdown and start-up periods. Historical Document 1997
Stress corrosion cracking (SCC) of RPV steels has shown fairly quick initiation and high crack growth rates (CGRs) in simulated normal water chemistry (NWC) autoclave tests. Still the operating experience shows no known cases that reflect this high sensitivity. The bulk of these tests have been conducted on either high sulfur material, with significant dynamic loading and/or in high sulphate or chloride environments. Recent studies at PSI and GE have shown increased CGRs at 3-5 ppb chloride. This led to the limit for normal operating conditions in the EPRI BWR water Chemistry Guidelines [3,4] to be reduced from 5 to 3 ppb of chloride during the course of this project. The effects on the in-crack chemistry of test specimens vs. those of real cracks, and the effect of cladding on cracking in LAS have been debated.
This standard practice provides mitigation methods to protect austenitic stainless steels and other austenitic alloys from polythionic acid (PTA) stress corrosion cracking (SCC) that can occur during a shutdown of refinery equipment. A shutdown includes the actual down time period and the contiguous periods required to shut down and start up the equipment.
Alloy 625 (UNS N06625) is an austenitic solid solution strengthened nickel-chromium-molybdenum alloy containing niobium. The high alloy content of alloy 625 enables it to withstand a wide variety of severe corrosive environments. In mild environments, such as ambient atmosphere, fresh and seawater, neutral salts and alkaline media, there is almost no attack.
Unexpected brittle failures of UNS NO5500 drill string parts and non-magnetic drill collars have recently been observed in cases where the UNS NO5500 components were galvanically coupled to carbon steel in concentrated salt solutions at temperatures between ambient and higher than 373 K. Cracking occured preferable at locations with a tri-axial stress condition (roots of threads) and has been ascribed to hydrogen embrittlement.
Stabilized austenitic stainless steel (SS) grade 347 is used extensively in high-temperature processes in the petroleum refining industry, while duplex SS (DSS) grade 2205 is a relatively newer material in the industry. Though these grades of SSs perform well in refinery process streams, there are incidents of failure of process equipment attributable to stress corrosion cracking (SCC). The paper deals with a study on the cracking susceptibility of SS grade 347 and DSS grade 2205 in refinery simulated process environments containing hydrogen sulfide and chloride. The paper also reports the electrochemical behavior of these SSs in the medium containing hydrogen sulfide and chloride. The electrochemical behavior of the alloys was assessed by cyclic polarization experiments. Slow strain rate test (SSRT) was used to evaluate the susceptibility of the alloys to SCC. The cyclic polarization studies indicate that the H2S – chloride synergism had a pronounced effect on the localized corrosion susceptibility of 347 SS, while the effect was marginal on the alloy DSS 2205. The SCC susceptibility of 347 SS and DSS 2205 is strongly influenced by hydrogen sulfide-chloride synergism. Initiation of corrosion pits and the sulfidation of active pits due to the synergism were the important steps in the initiation of SCC.
Slow strain rate (SSR) test method for screening and evaluating susceptibility of steels to ethanol Stress Corrosion Cracking (SCC). Relevent to the distribution of fuel ethanol.
This standard establishes a slow strain rate (SSR) test method for screening corrosion-resistant alloys (CRAs) (i.e., stainless steels and nickel-based alloys) for resistance to stress corrosion cracking (SCC) at elevated temperatures in sour oilfield production environments. The SSR test, which is relatively short in duration, incorporates a slow, dynamic strain applied at a constant extension rate. This results in acceleration of the initiation of cracking in susceptible materials, thereby simulating rather severe conditions.
The standard specifies reagents, test specimen, test equipment, determination of baseline material properties, environmental and mechanical test conditions, test procedure, and analysis and reporting of test results. It is intended for use by laboratory investigators for screening CRAs for resistance to SCC in sour oilfield service.
This revision extends the scope of the standard to address the screening of precipitation-hardened nickel-based alloys for resistance to hydrogen induced stress cracking (HISC) using the SSR test method.